SCI论文中常用的表达方法.docx

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SCI论文中常用的表达方法.docx

SCI论文中常用的表达方法

SCI论文中常用的表达方法

SCI论文写作中常用的表达方法

河北医科大学药学院天然药物教研室史清文教授

摘要:

要写好SCI论文,就需要建立一个适合自己需要的句型库(选择的词汇来源于SCI引用期刊论文Tetrahedron,TetrahedronLetterandJ.Nat.Prod,等)以及一些常用的各种核磁技术的文献。

本文根据自己体会以及多方资料整理(出处略),仅供研究生学习参考。

1引言部分(Introduction)

问题的提出;研究的现状及背景Background;以前工作基础;本工作的目的;思路(可提假说);合适的切入点,以探讨……(目的)等。

PreviousWork:

说明自己与前人的不同:

将历史上前人的工作分成类别;对每项重要的历史工作进行简短的回顾,要正确,抓住要点,避免歧义;和自己提出的工作进行比较;公正评价前人的重要工作,不要过于苛刻;强调自己的工作和前人工作的不同,特色。

引用参考文献:

立论依据的文献特别是新的和权威性文献,如:

Nature、Science、JACS、JOJ、OL等,还要引用自己的工作表明工作连续性。

OurWork:

描述自己的工作,回顾研究背景,常用词汇有review,outline,summarize,present,describe等。

说明写作目的:

常用词汇有purpose,attempt,aim等。

介绍论文的重点内容或研究范围:

常用词汇有study,present,emphasize,include,focus,attention,emphasis,investigation,inderline等。

Despitethemanyvaluablediscoveriesmadethroughstudiesof….,the…remainvirtuallyunexploredfromachemicalstandpoint.Interestingstructures(diversityofsecondarymetabolites)discoveredfromthe……promoted(stimulated)ustoundertakeaninvestigationonthe(attractedourinterestinthechemicalstudiesoforinitiatedtoexamine….)orinthepursuitofecologicallyimportantmetabolitesfrom…anunambiguousstructuraldeterminationofthemweredesired.在叙述前人成果之后,用However来引导不足,提出一种新方法或新方向(Indeed)。

如:

However,littleinformation(littleattention/littlework/littledata/littleresearch……)(orfewstudies/fewinvestigations/fewresearchers/fewattempts……)(orno/noneofthesestudies……)has(have)beendoneon(focusedon/attemptedto/conducted/investigated/studied(withrespectto))。

如:

Previousresearch(studies,records)has(have)failedtoconsider/ignored/misinterpreted/neglectedto/overestimated,underestimated/misleaded.Thus,thesepreviousresultsareinconclusive,misleading,unsatisfactory,questionable,controversial.Uncertainties(discrepancies)stillexist……

研究方法和方向与前人一样时,可通过以下方式强调自己工作:

However,dataisstillscarce(rare,lessaccurate)orthereisstilldearthof……Weneedto(aimto,haveto)providemore

documents(data,records,studies,increasethedataset).Furtherstudiesarestillnecessary(essential)……

提出自己的观点:

Weaimto/Thispaperreportson/Thispaperprovidesresults/Thispaperextendsthemethod/Thispaperfocuson……Thepurposeofthispaperisto……Furthermore,Moreover,Inaddition,wewillalsodiscuss……;Fromthechemicalpointofview,itisinterestingtounderlinethat….

2实验方法部分(Methods)

介绍研究或试验过程,常用词汇有:

test,study,analyze,investigate,examine,experiment,check,discuss,consider,analysis,ensure等。

说明研究或试验方法,常用词汇有:

measure,estimate,calculate等。

例:

GeneralExperimentalProcedures:

Solventsforextractionsandopencolumnchromatographywerereagent(analytical)gradeandusedwithoutfurtherpurification.Meltingpointsweredeterminedona…..apparatusandareuncorrected.

TheIRspectraweretakeninKBrpelletona...spectrophotometer.

OpticalrotationsweremeasuredusingaPerking-Elmermodel343digitalpolarimeterinchloroformat20°Cwithapathlengthof10cm(using10cmcelltube)recordedonthesodiumDline,usingasodiumlampoperatingat589nm.

UVspectrawererecorded(madeon)usingaJASCOmodelV-560UV/Visspectrophotometerinchloroform.

IRspectrawererun(performed)asthinfilmon(using)a….spectrophotometer.IRisindicativethepresencehydroxylgroup(abroadvibrationalbandaround3448cm-1)andacarbonylbandbetween1780-1658cm-1.

1Hand13CNMRspectrawereobtained(acquired)onaBrukermodelAMXorVarinUNITY500MHzspectrometerat500MHzfor1Hand125MHzfor13CinCDCl3assolventusingTMSasinternalstandard.CDCl3wasusedassolventandtetramethylsilane(TMS)asinternalstandard.Chemicalshiftswerereferencedrelativetothecorrespondingresidualsolventssignals(d

7.26/77.7,respectively)andaregivenonad(ppm)scaleandcouplingconstants(J)expressedinHz.Stereochemicaldesignationsandfollowingthechemicalshiftrefertotheprotonbelowandabovetheplane,respectively,oftheillustrateddrawing.Spin-coupledpatternsaredesignedasfollows:

s=singlet,d=doublet,t=triplet,q=quartet,m=multiplet,br=broadened,andh=hiddenoro=overlapped.Thespincouping(J)isgiveninparenthesesinHz,andreferstoseparationvaluessolelyforcharacterizationandmaynotbethetrueJasinnon-first-orderpatterns.SomehiddenpatternswereclarifiedbyhomonucleardecouplingandNOEstudiesandarereportedafterthehmdesignationinbrackets.Themultiplicitiesofthecarbonsignals(Methylene,

Methine,Methyl,orquternarycarbon)weredeterminedindirectlyfromHMQCexperiment.

HMQC[HeteronuclearMultipleQuantumCoherence,Bax,A.;Subramanian,S.J.Magn.Res.1986,67,565-569.]

HMBC[HeteronuclearMultipleBondCorrelation,Bax,A.;Summers,M.F.J.Am.Chem.Soc.1986,108,2093-2094.]

DEPT(DistortionlessEnhancementbyPolarizationTransfer)wasusedtosortCH3,CH2,CHand

C.

EI-MSweretaken(madeorobtained)onaMicromassmodelAutospec(70eV)spectrometer.AnalyticTLCwasperformedonprecoated0.25mmthickMerksilicagelF254aluminum-backedplateswithoutactivation.FractionswasmonitoredbyTLCwithvisualizationunderUVlight(254and365nm)andbydippingtheplatesintoasolutionof10%(v/v)H2SO4inEtOH.ThespotsweredetectedatUV(254nm)andvisualizedbysprayingwith5%H2SO4-ethanolreagentandheatingat140°C.

PreparedTLCwascarriedout(performed)onprecoatedSigel60F254plates(20´20cm,0.5mmlayerthickness,Merck).Developedchromatogramsweredetectedbysprayingwith10%H2SO4-ethanol,followedbyheatingat100°Cfor5min.PTLCplatewascutintosmallstripsunderUV,ThecompoundswerecarefullyremovedbyscrapingoffthesilicagelattheappropriateRfandthemwereexhaustivelyextractedwithacetonitrile.Aftersolventevaporation,theresiduewasusedtorunNMR.

SephadexLH-20column,previouslyequilibratedwithsamemixtureofelute,werealsoutilizedforfurtherseparation(MeOHorMeOH:

dichloromethane)aseluent(apolarextractusingMeOH:

CHCl3=1:

1,polarusingMeOH:

CHCl3=4:

1orMeOHonlyasmobilephase).

3实验结果讨论(DiscussionandSummary)

展示研究结果,常用词汇有:

show,result,disclose,present,displayed,infer等;介绍结论,常用词汇有introduce,summary,conclude,deduce等。

陈述论文的论点和作者的观点,常用词汇有:

report,suggest,expect,present,describe,argue等。

说明论证,常用词汇有:

support,provide,find,indicate,identify,confirm,clarify,demonstrate,imply,corroborate,evidence等。

推荐和建议,常用词汇有:

suggest,givesuggestion,recommendation,recommend,propose,necessity,expect,necessary,presume等。

例:

ResultandDiscussion:

UVabsorptionmaximaat315nmshowing(displayed)significantbathochromicshiftunderstrongalkalineconditions,indicating(wassupportive)thepresenceofphenolicfunctions

IRdatarevealedtheabsenceofabsorptionsforhydroxylgrouporunsaturation,suggestingthat

theoxygenisinvolvedinetherlinkagesandthatmoleculeistricyclic,etal.

FABMSspectrumrevealedthesodiumadduct(quasi-molecularion)[M+Na]+ionatm/zxx,suggestingMr=xxxandsolvingfor(Empiricalformula),whichwasappropriateforthemolecularformulaCxHyOz,ThismolecularformulawascorroboratedbyHR-FAB-MS,whichwasconsistentwithdatafrom1Hand13CNMRspectra.

1H-NMRspectrumdisplayedsignalscorrespondingtoprotons,whichareinthevicinityofheteroatoms.(showed(disclosed)atotalprotonsattachedtocarbon,indicatingthepresenceof…).Vicinalprotoncouplingconstantshavebeenveryusefulfortheconformationalanalysisofalargenumberoforganicsubstancesinviewoftheirknowndihedralangledependence.(Karplus,M.J.Chem.Phys.1959,30:

11.)

13C-NMRsignalscanbesorted(classified,defined)byDEPTexperimentsintomethyl,methylene,sp3methineandandsp2methineandsp3quaternarycarbon,sp2quaternarycarbonandoxygenatedsp2quaternarycarbonandcarbonylcarbon.DEPTexperimentsgroupedallofthecarbonsignalsintothefollowingassemblies:

1H-1HCOSYNMRspectrumwaspossibletodifferentiatehowmanydiscretedspinsystem.

HMBC(Bax,A.;Summers,M.F.J.Am.Chem.Soc.1986,108,2093-2094.):

Fullassignmentsoftheprotonandcarbonsignalsweresecuredby1H-1HDQFCOSY,HSQC,andHMBCspectra.Toclarifytheintermolecularconnectivitiesofthepartialstructures,theHMBCexperimentwasperformed.

1H-1HDQFCOSY(Piantini,U.;Sorensen,O.W.;Ernst,R.R.J.Am.Chem.Soc.1982,104,H-13CTOCSY(Braunschweiler,L.;Ernst,R.R.J.Magn.Reson.1983,53,521.)

C-13CTOCSY(Kjellerg,A.;Nishida,T.;Weitraub,A.;Widmalm,G.NMRSpectroscopyofC-Enrichedpolysaccharides:

Applicationof136800.)11313C-13CTOCSYtoSugarsofDifferentConfiguration.Magn.Reson.Chem.1998,35,128-131.)

Stereochemistry:

Therelativestereostructureof…asshowninacomputer-generated3Ddrawingwasdeducedfromcross-peaksobservedinthephase-sensitiveNOESYspectrumand3Jprotoncouplingconstants.Onthebasisoftheaboveargument,therelativestereochemistryof…wasassigned(determined,deduced,established,andcharacterized)as…

CD(CircularDichroism:

Berova,N.,Nakanishi,K.,Woody,R.W.,Eds.,CircularDichroism2nded.;Wiley-VCH:

NewYork,2000.)

Cytotoxicityassay-ThebioassayforcytotoxicitywasperformedbyMTT

[3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazoliumbromide]assay(TwentymanP.R.andLuscombeM.,Astudyofsomevariablesinatetrazoliumdye(MTT)basedassayforcellgrowthandchemosensitivity.Br.J.Cancer1987,56,279D285.)

对于推断出的结论,通常可用:

Resultsindicate,infer,suggest,implythat……,更肯定一点是可用:

Weconfirmthat……或Webelievethat……,偶尔也用:

Weputforward(discover,observe)……"forthefirsttime"来强调自己的创新。

如果自己对所提出的观点不完全肯定,可用:

Wetentativelyputforward(interpretthisto…),或Theresultsmaybeduet

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