SCI论文中常用的表达方法.docx
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SCI论文中常用的表达方法
SCI论文中常用的表达方法
SCI论文写作中常用的表达方法
河北医科大学药学院天然药物教研室史清文教授
摘要:
要写好SCI论文,就需要建立一个适合自己需要的句型库(选择的词汇来源于SCI引用期刊论文Tetrahedron,TetrahedronLetterandJ.Nat.Prod,等)以及一些常用的各种核磁技术的文献。
本文根据自己体会以及多方资料整理(出处略),仅供研究生学习参考。
1引言部分(Introduction)
问题的提出;研究的现状及背景Background;以前工作基础;本工作的目的;思路(可提假说);合适的切入点,以探讨……(目的)等。
PreviousWork:
说明自己与前人的不同:
将历史上前人的工作分成类别;对每项重要的历史工作进行简短的回顾,要正确,抓住要点,避免歧义;和自己提出的工作进行比较;公正评价前人的重要工作,不要过于苛刻;强调自己的工作和前人工作的不同,特色。
引用参考文献:
立论依据的文献特别是新的和权威性文献,如:
Nature、Science、JACS、JOJ、OL等,还要引用自己的工作表明工作连续性。
OurWork:
描述自己的工作,回顾研究背景,常用词汇有review,outline,summarize,present,describe等。
说明写作目的:
常用词汇有purpose,attempt,aim等。
介绍论文的重点内容或研究范围:
常用词汇有study,present,emphasize,include,focus,attention,emphasis,investigation,inderline等。
Despitethemanyvaluablediscoveriesmadethroughstudiesof….,the…remainvirtuallyunexploredfromachemicalstandpoint.Interestingstructures(diversityofsecondarymetabolites)discoveredfromthe……promoted(stimulated)ustoundertakeaninvestigationonthe(attractedourinterestinthechemicalstudiesoforinitiatedtoexamine….)orinthepursuitofecologicallyimportantmetabolitesfrom…anunambiguousstructuraldeterminationofthemweredesired.在叙述前人成果之后,用However来引导不足,提出一种新方法或新方向(Indeed)。
如:
However,littleinformation(littleattention/littlework/littledata/littleresearch……)(orfewstudies/fewinvestigations/fewresearchers/fewattempts……)(orno/noneofthesestudies……)has(have)beendoneon(focusedon/attemptedto/conducted/investigated/studied(withrespectto))。
如:
Previousresearch(studies,records)has(have)failedtoconsider/ignored/misinterpreted/neglectedto/overestimated,underestimated/misleaded.Thus,thesepreviousresultsareinconclusive,misleading,unsatisfactory,questionable,controversial.Uncertainties(discrepancies)stillexist……
研究方法和方向与前人一样时,可通过以下方式强调自己工作:
However,dataisstillscarce(rare,lessaccurate)orthereisstilldearthof……Weneedto(aimto,haveto)providemore
documents(data,records,studies,increasethedataset).Furtherstudiesarestillnecessary(essential)……
提出自己的观点:
Weaimto/Thispaperreportson/Thispaperprovidesresults/Thispaperextendsthemethod/Thispaperfocuson……Thepurposeofthispaperisto……Furthermore,Moreover,Inaddition,wewillalsodiscuss……;Fromthechemicalpointofview,itisinterestingtounderlinethat….
2实验方法部分(Methods)
介绍研究或试验过程,常用词汇有:
test,study,analyze,investigate,examine,experiment,check,discuss,consider,analysis,ensure等。
说明研究或试验方法,常用词汇有:
measure,estimate,calculate等。
例:
GeneralExperimentalProcedures:
Solventsforextractionsandopencolumnchromatographywerereagent(analytical)gradeandusedwithoutfurtherpurification.Meltingpointsweredeterminedona…..apparatusandareuncorrected.
TheIRspectraweretakeninKBrpelletona...spectrophotometer.
OpticalrotationsweremeasuredusingaPerking-Elmermodel343digitalpolarimeterinchloroformat20°Cwithapathlengthof10cm(using10cmcelltube)recordedonthesodiumDline,usingasodiumlampoperatingat589nm.
UVspectrawererecorded(madeon)usingaJASCOmodelV-560UV/Visspectrophotometerinchloroform.
IRspectrawererun(performed)asthinfilmon(using)a….spectrophotometer.IRisindicativethepresencehydroxylgroup(abroadvibrationalbandaround3448cm-1)andacarbonylbandbetween1780-1658cm-1.
1Hand13CNMRspectrawereobtained(acquired)onaBrukermodelAMXorVarinUNITY500MHzspectrometerat500MHzfor1Hand125MHzfor13CinCDCl3assolventusingTMSasinternalstandard.CDCl3wasusedassolventandtetramethylsilane(TMS)asinternalstandard.Chemicalshiftswerereferencedrelativetothecorrespondingresidualsolventssignals(d
7.26/77.7,respectively)andaregivenonad(ppm)scaleandcouplingconstants(J)expressedinHz.Stereochemicaldesignationsandfollowingthechemicalshiftrefertotheprotonbelowandabovetheplane,respectively,oftheillustrateddrawing.Spin-coupledpatternsaredesignedasfollows:
s=singlet,d=doublet,t=triplet,q=quartet,m=multiplet,br=broadened,andh=hiddenoro=overlapped.Thespincouping(J)isgiveninparenthesesinHz,andreferstoseparationvaluessolelyforcharacterizationandmaynotbethetrueJasinnon-first-orderpatterns.SomehiddenpatternswereclarifiedbyhomonucleardecouplingandNOEstudiesandarereportedafterthehmdesignationinbrackets.Themultiplicitiesofthecarbonsignals(Methylene,
Methine,Methyl,orquternarycarbon)weredeterminedindirectlyfromHMQCexperiment.
HMQC[HeteronuclearMultipleQuantumCoherence,Bax,A.;Subramanian,S.J.Magn.Res.1986,67,565-569.]
HMBC[HeteronuclearMultipleBondCorrelation,Bax,A.;Summers,M.F.J.Am.Chem.Soc.1986,108,2093-2094.]
DEPT(DistortionlessEnhancementbyPolarizationTransfer)wasusedtosortCH3,CH2,CHand
C.
EI-MSweretaken(madeorobtained)onaMicromassmodelAutospec(70eV)spectrometer.AnalyticTLCwasperformedonprecoated0.25mmthickMerksilicagelF254aluminum-backedplateswithoutactivation.FractionswasmonitoredbyTLCwithvisualizationunderUVlight(254and365nm)andbydippingtheplatesintoasolutionof10%(v/v)H2SO4inEtOH.ThespotsweredetectedatUV(254nm)andvisualizedbysprayingwith5%H2SO4-ethanolreagentandheatingat140°C.
PreparedTLCwascarriedout(performed)onprecoatedSigel60F254plates(20´20cm,0.5mmlayerthickness,Merck).Developedchromatogramsweredetectedbysprayingwith10%H2SO4-ethanol,followedbyheatingat100°Cfor5min.PTLCplatewascutintosmallstripsunderUV,ThecompoundswerecarefullyremovedbyscrapingoffthesilicagelattheappropriateRfandthemwereexhaustivelyextractedwithacetonitrile.Aftersolventevaporation,theresiduewasusedtorunNMR.
SephadexLH-20column,previouslyequilibratedwithsamemixtureofelute,werealsoutilizedforfurtherseparation(MeOHorMeOH:
dichloromethane)aseluent(apolarextractusingMeOH:
CHCl3=1:
1,polarusingMeOH:
CHCl3=4:
1orMeOHonlyasmobilephase).
3实验结果讨论(DiscussionandSummary)
展示研究结果,常用词汇有:
show,result,disclose,present,displayed,infer等;介绍结论,常用词汇有introduce,summary,conclude,deduce等。
陈述论文的论点和作者的观点,常用词汇有:
report,suggest,expect,present,describe,argue等。
说明论证,常用词汇有:
support,provide,find,indicate,identify,confirm,clarify,demonstrate,imply,corroborate,evidence等。
推荐和建议,常用词汇有:
suggest,givesuggestion,recommendation,recommend,propose,necessity,expect,necessary,presume等。
例:
ResultandDiscussion:
UVabsorptionmaximaat315nmshowing(displayed)significantbathochromicshiftunderstrongalkalineconditions,indicating(wassupportive)thepresenceofphenolicfunctions
IRdatarevealedtheabsenceofabsorptionsforhydroxylgrouporunsaturation,suggestingthat
theoxygenisinvolvedinetherlinkagesandthatmoleculeistricyclic,etal.
FABMSspectrumrevealedthesodiumadduct(quasi-molecularion)[M+Na]+ionatm/zxx,suggestingMr=xxxandsolvingfor(Empiricalformula),whichwasappropriateforthemolecularformulaCxHyOz,ThismolecularformulawascorroboratedbyHR-FAB-MS,whichwasconsistentwithdatafrom1Hand13CNMRspectra.
1H-NMRspectrumdisplayedsignalscorrespondingtoprotons,whichareinthevicinityofheteroatoms.(showed(disclosed)atotalprotonsattachedtocarbon,indicatingthepresenceof…).Vicinalprotoncouplingconstantshavebeenveryusefulfortheconformationalanalysisofalargenumberoforganicsubstancesinviewoftheirknowndihedralangledependence.(Karplus,M.J.Chem.Phys.1959,30:
11.)
13C-NMRsignalscanbesorted(classified,defined)byDEPTexperimentsintomethyl,methylene,sp3methineandandsp2methineandsp3quaternarycarbon,sp2quaternarycarbonandoxygenatedsp2quaternarycarbonandcarbonylcarbon.DEPTexperimentsgroupedallofthecarbonsignalsintothefollowingassemblies:
1H-1HCOSYNMRspectrumwaspossibletodifferentiatehowmanydiscretedspinsystem.
HMBC(Bax,A.;Summers,M.F.J.Am.Chem.Soc.1986,108,2093-2094.):
Fullassignmentsoftheprotonandcarbonsignalsweresecuredby1H-1HDQFCOSY,HSQC,andHMBCspectra.Toclarifytheintermolecularconnectivitiesofthepartialstructures,theHMBCexperimentwasperformed.
1H-1HDQFCOSY(Piantini,U.;Sorensen,O.W.;Ernst,R.R.J.Am.Chem.Soc.1982,104,H-13CTOCSY(Braunschweiler,L.;Ernst,R.R.J.Magn.Reson.1983,53,521.)
C-13CTOCSY(Kjellerg,A.;Nishida,T.;Weitraub,A.;Widmalm,G.NMRSpectroscopyofC-Enrichedpolysaccharides:
Applicationof136800.)11313C-13CTOCSYtoSugarsofDifferentConfiguration.Magn.Reson.Chem.1998,35,128-131.)
Stereochemistry:
Therelativestereostructureof…asshowninacomputer-generated3Ddrawingwasdeducedfromcross-peaksobservedinthephase-sensitiveNOESYspectrumand3Jprotoncouplingconstants.Onthebasisoftheaboveargument,therelativestereochemistryof…wasassigned(determined,deduced,established,andcharacterized)as…
CD(CircularDichroism:
Berova,N.,Nakanishi,K.,Woody,R.W.,Eds.,CircularDichroism2nded.;Wiley-VCH:
NewYork,2000.)
Cytotoxicityassay-ThebioassayforcytotoxicitywasperformedbyMTT
[3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazoliumbromide]assay(TwentymanP.R.andLuscombeM.,Astudyofsomevariablesinatetrazoliumdye(MTT)basedassayforcellgrowthandchemosensitivity.Br.J.Cancer1987,56,279D285.)
对于推断出的结论,通常可用:
Resultsindicate,infer,suggest,implythat……,更肯定一点是可用:
Weconfirmthat……或Webelievethat……,偶尔也用:
Weputforward(discover,observe)……"forthefirsttime"来强调自己的创新。
如果自己对所提出的观点不完全肯定,可用:
Wetentativelyputforward(interpretthisto…),或Theresultsmaybeduet