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中文翻译材料
FractureToughnessofSi3N4/S45CJointwithanInterfaceCrack
LiedongFu,YukioMiyasitaandYoshiharuMutoh
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Posted:
September2005
TopicsCovered
Abstract
FracturetoughnesstestswerecarriedoutforSi3N4/S45Cspecimenswithinterfacecracksofdifferentlengths. Itwasfoundthatthespecimenwithacrackof4mmhashigherapparentfracturetoughnessthanthosewithcracksof1mmand2mmduetothereductionoftheresidualstress. FracturepropagatedintoSi3N4 fromthecracktipinthedirectionof40o forcracksof1mmand2mmwhileitpropagatedalongtheinterfaceforcrackof4mm. Elasto-plasticanalysiswascarriedoutconsideringS45CasthelinearhardeningmaterialandSi3N4 astheelasticmaterial. Itwasfoundthatthestressaroundthecracktipisdominatedbyanelasto-plasticsingularstressfield,whichissubstantiallythesameastheelasticsingularstressfieldofaninterfacecrack. Evaluationofthefracturepathandtoughnesswascarriedoutbasedonthestressintensityfactorsoftheelasto-plasticsingularstressfield.
Keywords
InterfaceCrack,FractureToughness,Si3N4/S45CJoint,ThermalResidualStress,Elasto-plasticAnalysis
Introduction
Theceramic/metaljointshavebeenincreasinglyappliedinawiderangeofengineeringfieldsbecausetheceramichasstablemechanicalpropertiesathightemperatureandgoodresistancetowear,erosionandoxidation. However,thedifferenceofmaterialpropertiesbetweenmetalandceramicinducesstresssingularitiesattheinterfaceedge. Moreover,highthermalresidualstresswillbeinducedduringthecoolingprocessduetothemismatchofthethermalexpansioncoefficients. Thestresssingularitytogetherwiththethermalresidualstressdegradesthestrengthofceramic/metaljointandmakestheevaluationofthestrengthdifficult. Manyworkshavebeendoneabouttheresidualstressandthestrengthevaluationofceramic/metaljoints. Forexample,Kobayashietal.[1,2]haveinvestigatedthebendingstrengthandresidualstressofSi3N4/S45Cjointandtheeffectofthesizeofthespecimenonthebendingstrength. Qiuetal.[3]haveinvestigatedtheinfluenceofresidualstressandcyclicloadonthestrengthofSi3N4/S45Cjoint. However,duetothecomplexityoftheproblem,ageneralizedevaluationmethodfortheceramic/metaljointhasnotyetbeenproposed.
Theelasticsolutionofthesingularstressfieldoftheinterfacecrackhasbeenstudiedsince1959[4-9]. Rice[10]hassummarizedtheworkinthisfieldandsetuptheelasticfracturemechanicsconceptsforinterfacialcracks. Yuukietal.[11,12]haveproposedthemaximumnormalstresscriteriaforpredictingfracturepathandstrengthofceramic/metaljointbasedontheelasticplasticdeformationofmetalwillinevitablyappearnearthecracktipduetothestresssingularity. Formostoftheceramic/metaljoints,theplasticdeformationofmetalhasasignificantinfluenceonthestrengthoftheceramic/metaljoint. Duetotheanalyticalcomplexity,theevaluationofthefracturepathandstrengthofceramic/metaljointbasedontheelasto-plastictheoryhasnotyetbeenmade.
Inthisstudy,fourpointbendingtestsofSi3N4/S45Cjointspecimenswithaninterfacecrackwerecarriedout. Evaluationofthefracturepathandfracturetoughnesswasattemptedbasedontheelasto-plasticanalysis.
Experimental
Specimen Preparation
Figure1showsthegeometryanddimensionsofSi3N4/S45Cjointspecimen. Thesilverbasedbrazingalloy(wt%is:
Ag,71%,Cu,27%,Ti,2%)with60μmthicknesswasusedforthebondingbetweenSi3N4 ceramicsandS45Csteel. Brazingwascarriedinavacuumfurnace Torr). Thetemperatureofthefurnacewasincreasedatarateof20oC/minuptothebrazingtemperatureof850oCandkeptfor10min,thendecreasedatarateof10oC/min. Thejoiningsurfaceswerepolishedwithdiamondpowderofμmdiameter. Duringthebrazing,acontactpressureofMPawasapplied.
Afterbrazing,aninterfacecrackwasintroducedbytheelectricdischargemethodwiththecuttingwireof0.1mmdiameter. Fourspecimenswithdifferentcracklengthswereprepared. Twoofthespecimenshadcracklengthsof4.0mmandtheothertwospecimenshadcracklengthsof1.0mmand2.0mm.
Figure1. Fracturetoughnessspecimen.
ExperimentalResults
Fourpointbendingtestswerecarriedoutonthefracturetoughnessspecimensatacrossheadspeedof0.5mm/min. Table1showstheresultsofthefracturetoughness. Theapparentfracturetoughnessisdefinedas:
(1)
with
(2)
(3)
WherePf isthefractureload,aisthecracklength,wthespecimenwidth,tthespecimenhighness,L2 theouterspanandL1 theinnerspan.
Table1. Resultofthefracturetoughnesstests.
No.
Cracklengtha(mm)
Pf (N)
σ f (MPa)
FI
KIApparent(MPa√m)
1
2
3
4
AscanbeseeninTable1,thespecimenswithacracklengthof4.0mmindicateahigherfractureloadthanthosewithshortercracklengthsofand2.0mm. Astheresidualstresswillredistributeaftercutting[2],therelaxationofthermalresidualstressforlongercracklengthmaybeapossiblereason.
Figure2showsthemacroscopicobservationofthefracturedspecimen. Forthespecimenswithacracklengthofand2.0mm,crackpropagatedintoSi3N4 directlyfromtheinitialcracktipinthedirectionofabout40o. Forthespecimenswithacracklengthof4.0mm,thecrackpropagatedalongtheinterfaceforabout1.0mmandthenkinkedintoSi3N4 inadirectionofabout10o totheinterface.
(a)a=1.0mm
(b)a=2.0mm
(c)a=4.0mm
(d)a=4.0mm
Figure2. Fracturedspecimens.
OscillatorySingularStressFieldofTheInterfaceCrackandTheMaximumNormalStressCriteria
TheelasticsolutionofthestressfieldofaninterfacecrackhasbeenaccomplishedbytheWillims[4],Erdogan[5,6],England[7]andSihetal.[8,9]. Ithasbeenfoundthatthestressfieldneartheinterfacecracktiphastheoscillatorysingularity. Underthepolarcoordinatewiththeoriginlocatedatthecracktip,thestressfieldcanbeexpressedas
(4)
Here
isthebi-materialconstantthatcanbeexpressedas
(5)
(6)
whereµj and vj aretheshearmodulusandthePoisson’sratioofthematerials,respectively.
Thestressintensityfactorsoftheoscillatorysingularstressfieldaredefinedas
(7)
where, l isthereferencelengthtoeliminatethedimensionoftheoscillatoryterm. Usually l takesthevalueofthewholecracklength,.l=2a.
Whenthestressalongtheinterfacehasbeenknown,thestressintensityfactorscanbecanbeextrapolatedas:
(8)
(9)
Yuukietal.[11,12]haveproposedupthemaximumnormalstresscriteriaforthefractureofinterfacecrack. Consideringthatthevalueof
isverysmall,thenormalstresscanbeapproximatelyexpressedas
(10)
where
(11)
W1=e-ε(π-θ),W2=eε(π+θ) (12)
(13)
Thedirectionofthemaximumnormalstresscanbedeterminedfrom:
∂B(θ,ε,y)/∂θ=0 (14)
Letθ0 representthedirectionofthemaximumnormalstress,thecorrespondingstressintensityfactorcanbeexpressedas:
(15)
Fracturewilloccuralongthedirectionof θ0 whenKθmax reachestheKIC valueofthebasematerial. Itshouldbenotedthatfracturemayoccuralongtheinterfacewhen θ0 becomessmallerthancertainvalue,sincethestrengthofinterfaceisusuallylowerthanthatofthebasematerial.
Elasto-PlasticSingularStressFieldatTheInterfaceCrackTip
Theelasto-plasticsingularstressfieldforalinearhardeningmaterial[13]hasbeenfoundtobesubstantiallythesameasthatofelasticmaterialwhoseelasticconstantsaredefinedas:
(16)
whereEistheYoung’smodulusandH’thehardeningcoefficient.
Therefore,theelasto-plasticsingularstressfieldattheinterfacecracktipissubstantiallythesameastheelasticsingularstressfieldoftheinterfacecracktip. Thegoverningregionoftheelasto-plasticsingularstressfieldwillbeconfinedinasmallregionaroundthecracktipinsidetheyieldzone. Forceramic/metaljoint,consideringthatthevalueofhardeningcoefficientismuchlessthanthevalueofYoung’smodulus,itcanbefoundfromEq.(16)andEq.(5)that
(17)
FEMAnalysisandEvaluationofFracturePathandToughnessBasedontheElasto-PlasticStressIntensityFactors
FEManalysiswascarriedoutunderplanestressconditionusingtheprogramofABAQUS. Si3N4 isassumedasanelasticmaterialwhosematerialconstantsareindependentoftemperatureandE=289GPa, v=andCTE=. S45CsteelisassumedasalinearhardeningmaterialwiththematerialconstantslistedinTable2[14]. Thestressfreetemperatureisconsideredtobe550oCfortheanalysisofthethermalresidualstress.
Table2. MaterialconstantsofS45C
25oC
100oC
200oC
300oC
400oC
500oC
600oC
E (GPa)
206
206
201
197
192
187
183
v
σY- (MPa)
375
348
333
309
280
241
193
H’(MPa)
1381
2056
2680
2325
1685
1026
687
CTE(10-6)
Forcomparison,theelasticanalysiswasalsocarriedout. Calculatedfromtheelasticconstantsof25oC,thebi-materialconstant
forelasticcaseis. Table3liststhestressintensityfactorsaswellasthedirect