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中文翻译材料

FractureToughnessofSi3N4/S45CJointwithanInterfaceCrack

LiedongFu,YukioMiyasitaandYoshiharuMutoh

CopyrightAD-TECH.;licenseePtyLtd.

ThisisanAZoOpenAccessRewardsSystem(AZo-OARS)articledistributedunderthetermsoftheAZo–OARS  whichpermitsunrestricteduseprovidedtheoriginalworkisproperlycitedbutislimitedtonon-commercialdistributionandreproduction.

Posted:

September2005

TopicsCovered

 

Abstract

FracturetoughnesstestswerecarriedoutforSi3N4/S45Cspecimenswithinterfacecracksofdifferentlengths.  Itwasfoundthatthespecimenwithacrackof4mmhashigherapparentfracturetoughnessthanthosewithcracksof1mmand2mmduetothereductionoftheresidualstress.  FracturepropagatedintoSi3N4 fromthecracktipinthedirectionof40o forcracksof1mmand2mmwhileitpropagatedalongtheinterfaceforcrackof4mm. Elasto-plasticanalysiswascarriedoutconsideringS45CasthelinearhardeningmaterialandSi3N4 astheelasticmaterial.  Itwasfoundthatthestressaroundthecracktipisdominatedbyanelasto-plasticsingularstressfield,whichissubstantiallythesameastheelasticsingularstressfieldofaninterfacecrack.  Evaluationofthefracturepathandtoughnesswascarriedoutbasedonthestressintensityfactorsoftheelasto-plasticsingularstressfield.

Keywords

InterfaceCrack,FractureToughness,Si3N4/S45CJoint,ThermalResidualStress,Elasto-plasticAnalysis

Introduction

Theceramic/metaljointshavebeenincreasinglyappliedinawiderangeofengineeringfieldsbecausetheceramichasstablemechanicalpropertiesathightemperatureandgoodresistancetowear,erosionandoxidation. However,thedifferenceofmaterialpropertiesbetweenmetalandceramicinducesstresssingularitiesattheinterfaceedge.  Moreover,highthermalresidualstresswillbeinducedduringthecoolingprocessduetothemismatchofthethermalexpansioncoefficients.  Thestresssingularitytogetherwiththethermalresidualstressdegradesthestrengthofceramic/metaljointandmakestheevaluationofthestrengthdifficult.  Manyworkshavebeendoneabouttheresidualstressandthestrengthevaluationofceramic/metaljoints.  Forexample,Kobayashietal.[1,2]haveinvestigatedthebendingstrengthandresidualstressofSi3N4/S45Cjointandtheeffectofthesizeofthespecimenonthebendingstrength.  Qiuetal.[3]haveinvestigatedtheinfluenceofresidualstressandcyclicloadonthestrengthofSi3N4/S45Cjoint.  However,duetothecomplexityoftheproblem,ageneralizedevaluationmethodfortheceramic/metaljointhasnotyetbeenproposed.

Theelasticsolutionofthesingularstressfieldoftheinterfacecrackhasbeenstudiedsince1959[4-9].  Rice[10]hassummarizedtheworkinthisfieldandsetuptheelasticfracturemechanicsconceptsforinterfacialcracks.  Yuukietal.[11,12]haveproposedthemaximumnormalstresscriteriaforpredictingfracturepathandstrengthofceramic/metaljointbasedontheelasticplasticdeformationofmetalwillinevitablyappearnearthecracktipduetothestresssingularity.  Formostoftheceramic/metaljoints,theplasticdeformationofmetalhasasignificantinfluenceonthestrengthoftheceramic/metaljoint.  Duetotheanalyticalcomplexity,theevaluationofthefracturepathandstrengthofceramic/metaljointbasedontheelasto-plastictheoryhasnotyetbeenmade.

Inthisstudy,fourpointbendingtestsofSi3N4/S45Cjointspecimenswithaninterfacecrackwerecarriedout.  Evaluationofthefracturepathandfracturetoughnesswasattemptedbasedontheelasto-plasticanalysis.

Experimental

Specimen Preparation

Figure1showsthegeometryanddimensionsofSi3N4/S45Cjointspecimen. Thesilverbasedbrazingalloy(wt%is:

Ag,71%,Cu,27%,Ti,2%)with60μmthicknesswasusedforthebondingbetweenSi3N4 ceramicsandS45Csteel. Brazingwascarriedinavacuumfurnace Torr).  Thetemperatureofthefurnacewasincreasedatarateof20oC/minuptothebrazingtemperatureof850oCandkeptfor10min,thendecreasedatarateof10oC/min.  Thejoiningsurfaceswerepolishedwithdiamondpowderofμmdiameter. Duringthebrazing,acontactpressureofMPawasapplied.

Afterbrazing,aninterfacecrackwasintroducedbytheelectricdischargemethodwiththecuttingwireof0.1mmdiameter.  Fourspecimenswithdifferentcracklengthswereprepared.  Twoofthespecimenshadcracklengthsof4.0mmandtheothertwospecimenshadcracklengthsof1.0mmand2.0mm.

Figure1. Fracturetoughnessspecimen.

ExperimentalResults

Fourpointbendingtestswerecarriedoutonthefracturetoughnessspecimensatacrossheadspeedof0.5mm/min.  Table1showstheresultsofthefracturetoughness.  Theapparentfracturetoughnessisdefinedas:

                 

(1)

with

                 

(2)

                (3)

WherePf isthefractureload,aisthecracklength,wthespecimenwidth,tthespecimenhighness,L2 theouterspanandL1 theinnerspan.

Table1. Resultofthefracturetoughnesstests.

No.

Cracklengtha(mm)

Pf (N)

σ f (MPa)

FI

KIApparent(MPa√m)

1

2

3

4

AscanbeseeninTable1,thespecimenswithacracklengthof4.0mmindicateahigherfractureloadthanthosewithshortercracklengthsofand2.0mm.  Astheresidualstresswillredistributeaftercutting[2],therelaxationofthermalresidualstressforlongercracklengthmaybeapossiblereason.

Figure2showsthemacroscopicobservationofthefracturedspecimen.  Forthespecimenswithacracklengthofand2.0mm,crackpropagatedintoSi3N4 directlyfromtheinitialcracktipinthedirectionofabout40o.  Forthespecimenswithacracklengthof4.0mm,thecrackpropagatedalongtheinterfaceforabout1.0mmandthenkinkedintoSi3N4 inadirectionofabout10o totheinterface.

(a)a=1.0mm

(b)a=2.0mm

(c)a=4.0mm

(d)a=4.0mm

Figure2. Fracturedspecimens.

OscillatorySingularStressFieldofTheInterfaceCrackandTheMaximumNormalStressCriteria

TheelasticsolutionofthestressfieldofaninterfacecrackhasbeenaccomplishedbytheWillims[4],Erdogan[5,6],England[7]andSihetal.[8,9].  Ithasbeenfoundthatthestressfieldneartheinterfacecracktiphastheoscillatorysingularity.  Underthepolarcoordinatewiththeoriginlocatedatthecracktip,thestressfieldcanbeexpressedas

                (4)

Here 

 isthebi-materialconstantthatcanbeexpressedas

               (5)

             (6)

whereµj and vj aretheshearmodulusandthePoisson’sratioofthematerials,respectively.

Thestressintensityfactorsoftheoscillatorysingularstressfieldaredefinedas

               (7)

where, l isthereferencelengthtoeliminatethedimensionoftheoscillatoryterm.  Usually l takesthevalueofthewholecracklength,.l=2a.

Whenthestressalongtheinterfacehasbeenknown,thestressintensityfactorscanbecanbeextrapolatedas:

               (8)

              (9)

Yuukietal.[11,12]haveproposedupthemaximumnormalstresscriteriaforthefractureofinterfacecrack.  Consideringthatthevalueof 

 isverysmall,thenormalstresscanbeapproximatelyexpressedas

              (10)

where

           (11)

W1=e-ε(π-θ),W2=eε(π+θ)                (12)

                 (13)

Thedirectionofthemaximumnormalstresscanbedeterminedfrom:

∂B(θ,ε,y)/∂θ=0           (14)

Letθ0 representthedirectionofthemaximumnormalstress,thecorrespondingstressintensityfactorcanbeexpressedas:

               (15)

Fracturewilloccuralongthedirectionof θ0 whenKθmax reachestheKIC valueofthebasematerial.  Itshouldbenotedthatfracturemayoccuralongtheinterfacewhen θ0 becomessmallerthancertainvalue,sincethestrengthofinterfaceisusuallylowerthanthatofthebasematerial.

Elasto-PlasticSingularStressFieldatTheInterfaceCrackTip

Theelasto-plasticsingularstressfieldforalinearhardeningmaterial[13]hasbeenfoundtobesubstantiallythesameasthatofelasticmaterialwhoseelasticconstantsaredefinedas:

            (16)

whereEistheYoung’smodulusandH’thehardeningcoefficient.

Therefore,theelasto-plasticsingularstressfieldattheinterfacecracktipissubstantiallythesameastheelasticsingularstressfieldoftheinterfacecracktip.  Thegoverningregionoftheelasto-plasticsingularstressfieldwillbeconfinedinasmallregionaroundthecracktipinsidetheyieldzone.  Forceramic/metaljoint,consideringthatthevalueofhardeningcoefficientismuchlessthanthevalueofYoung’smodulus,itcanbefoundfromEq.(16)andEq.(5)that

        (17)

FEMAnalysisandEvaluationofFracturePathandToughnessBasedontheElasto-PlasticStressIntensityFactors

FEManalysiswascarriedoutunderplanestressconditionusingtheprogramofABAQUS.  Si3N4 isassumedasanelasticmaterialwhosematerialconstantsareindependentoftemperatureandE=289GPa, v=andCTE=.  S45CsteelisassumedasalinearhardeningmaterialwiththematerialconstantslistedinTable2[14].  Thestressfreetemperatureisconsideredtobe550oCfortheanalysisofthethermalresidualstress.

Table2. MaterialconstantsofS45C

 

25oC

100oC

200oC

300oC

400oC

500oC

600oC

E  (GPa)

206

206

201

197

192

187

183

v

σY- (MPa)

375

348

333

309

280

241

193

H’(MPa)

1381

2056

2680

2325

1685

1026

687

CTE(10-6)

Forcomparison,theelasticanalysiswasalsocarriedout.  Calculatedfromtheelasticconstantsof25oC,thebi-materialconstant

forelasticcaseis.  Table3liststhestressintensityfactorsaswellasthedirect

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