美国药典USP中规定的色谱柱类型Word格式.docx

美国药典USP中规定的色谱柱类型Word格式.docx

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mindiameter,oramonolithicsilicarod.

L2—Octadecylsilanechemicallybondedtosilicagelofacontrolledsurfaceporositythathasbeenbondedtoasolidsphericalcore,30to50&

mindiameter.

L3—Poroussilicaparticles,3USP31to10&

mindiameter,oramonolithicsilicarod.USP31

L4—Silicagelofcontrolledsurfaceporositybondedtoasolidsphericalcore,30to50&

L5—Aluminaofcontrolledsurfaceporositybondedtoasolidsphericalcore,30to50&

L6—Strongcation-exchangepacking–sulfonatedfluorocarbonpolymercoatedonasolidsphericalcore,30to50&

L7—Octylsilanechemicallybondedtototallyporoussilicaparticles,1.5to10&

L8—Anessentiallymonomolecularlayerofaminopropylsilanechemicallybondedtototallyporoussilicagelsupport,3to10&

L9—Irregularorspherical,totallyporoussilicagelhavingachemicallybonded,stronglyacidiccation-exchangecoating,3to10&

L10—Nitrilegroupschemicallybondedtoporoussilicaparticles,3to10&

L11—Phenylgroupschemicallybondedtoporoussilicaparticles,1.5to10&

L12—Astronganion-exchangepackingmadebychemicallybondingaquaternaryaminetoasolidsilicasphericalcore,30to50&

L13—Trimethylsilanechemicallybondedtoporoussilicaparticles,3to10&

L14—Silicagelhavingachemicallybonded,stronglybasicquaternaryammoniumanion-exchangecoating,5to10&

L15—Hexylsilanechemicallybondedtototallyporoussilicaparticles,3to10&

L16—Dimethylsilanechemicallybondedtoporoussilicaparticles,5to10&

L17—Strongcation-exchangeresinconsistingofsulfonatedcross-linkedstyrene-divinylbenzenecopolymerinthehydrogenform,7to11&

L18—Aminoandcyanogroupschemicallybondedtoporoussilicaparticles,3to10&

L19—Strongcation-exchangeresinconsistingofsulfonatedcross-linkedstyrene-divinylbenzenecopolymerinthecalciumform,about9&

L20—Dihydroxypropanegroupschemicallybondedtoporoussilicaparticles,5to10&

L21—Arigid,sphericalstyrene-divinylbenzenecopolymer,5to10&

L22—Acation-exchangeresinmadeofporouspolystyrenegelwithsulfonicacidgroups,about10&

minsize.

L23—Ananion-exchangeresinmadeofporouspolymethacrylateorpolyacrylategelwithquaternaryammoniumgroups,about10&

L24—Asemi-rigidhydrophilicgelconsistingofvinylpolymerswithnumeroushydroxylgroupsonthematrixsurface,32to63&

mindiameter.

[note—AvailableasYMC-PackPVA-SILmanufacturedbyYMCCo.,Ltd.anddistributedbyWatersCorp.（）.]

L25—Packinghavingthecapacitytoseparatecompoundswithamolecularweightrangefrom100–5000（asdeterminedbypolyethyleneoxide）,appliedtoneutral,anionic,andcationicwater-solublepolymers.Apolymethacrylateresinbase,cross-linkedwithpolyhydroxylatedether（surfacecontainedsomeresidualcarboxylfunctionalgroups）wasfoundsuitable.

L26—Butylsilanechemicallybondedtototallyporoussilicaparticles,3to10&

L27—Poroussilicaparticles,30to50&

L28—Amultifunctionalsupport,whichconsistsofahighpurity,100,sphericalsilicasubstratethathasbeenbondedwithanionicexchanger,aminefunctionalityinadditiontoaconventionalreversedphaseC8functionality.

L29—Gammaalumina,reverse-phase,lowcarbonpercentagebyweight,alumina-basedpolybutadienesphericalparticles,5&

mindiameterwithaporevolumeof80.

L30—Ethylsilanechemicallybondedtototallyporoussilicaparticles,3to10&

L31—Ahydroxide-selective,stronganion-exchangeresin-quaternaryaminebondedonlatexparticlesattachedtoacoreof8.5-&

mmacroporousparticleshavingaporesizeof2000andconsistingofethylvinylbenzenecross-linkedwith55%divinylbenzene.

L32—Achiralligand-exchangepacking–l-prolinecoppercomplexcovalentlybondedtoirregularlyshapedsilicaparticles,5to10&

L33—Packinghavingthecapacitytoseparatedextransbymolecularsizeoverarangeof4,000to500,000Da.Itisspherical,silica-based,andprocessedtoprovidepHstability.

[note—AvailableasTSKgelG4000SWXLfromTosohBiosep（）.]

L34—Strongcation-exchangeresinconsistingofsulfonatedcross-linkedstyrene-divinylbenzenecopolymerintheleadform,about9&

L35—Azirconium-stabilizedsphericalsilicapackingwithahydrophilic（diol-type）molecularmonolayerbondedphasehavingaporesizeof150.

L36—A3,5-dinitrobenzoylderivativeofl-phenylglycinecovalentlybondedto5-&

maminopropylsilica.

L37—Packinghavingthecapacitytoseparateproteinsbymolecularsizeoverarangeof2,000to40,000Da.Itisapolymethacrylategel.

L38—Amethacrylate-basedsize-exclusionpackingforwater-solublesamples.

L39—Ahydrophilicpolyhydroxymethacrylategeloftotallyporoussphericalresin.

L40—Cellulosetris-3,5-dimethylphenylcarbamatecoatedporoussilicaparticles,5to20&

L41—Immobilized1-acidglycoproteinonsphericalsilicaparticles,5&

L42—Octylsilaneandoctadecylsilanegroupschemicallybondedtoporoussilicaparticles,5&

L43—Pentafluorophenylgroupschemicallybondedtosilicaparticlesbyapropylspacer,5to10&

L44—Amultifunctionalsupport,whichconsistsofahighpurity,60,sphericalsilicasubstratethathasbeenbondedwithacationicexchanger,sulfonicacidfunctionalityinadditiontoaconventionalreversedphaseC8functionality.

L45—Betacyclodextrinbondedtoporoussilicaparticles,5to10&

L46—Polystyrene/divinylbenzenesubstrateagglomeratedwithquaternaryaminefunctionalizedlatexbeads,about10&

L47—High-capacityanion-exchangemicroporoussubstrate,fullyfunctionalizedwithtrimethlyaminegroups,8&

[note—AvailableasCarboPacMA1anddistributedbyDionexCorp.（）.]

L48—Sulfonated,cross-linkedpolystyrenewithanouterlayerofsubmicron,porous,anion-exchangemicrobeads,15&

L49—Areversed-phasepackingmadebycoatingathinlayerofpolybutadieneontosphericalporouszirconiaparticles,3to10&

[note—AvailableasZirchromPBD,manufacturedbyZirChromSeparations,Inc.,distributedbyAlltech,www.A.]

L50—Multifunctionresinwithreversed-phaseretentionandstronganion-exchangefunctionalities.Theresinconsistsofethylvinylbenzene,55%cross-linkedwithdivinylbenzenecopolymer,3to15&

mindiameter,andasurfaceareanotlessthan350m2perg.Substrateiscoatedwithquaternaryammoniumfunctionalizedlatexparticlesconsistingofstyrenecross-linkedwithdivinylbenzene.

[note—AvailableasOmniPacPAX-500anddistributedbyDionexCorp.（）.]

L51—Amylosetris-3,5-dimethylphenylcarbamate-coated,porous,spherical,silicaparticles,5to10&

[note—AvailableasChiralpakADfromChiralTechnologies,Inc.,（）.]

L52—Astrongcation-exchangeresinmadeofporoussilicawithsulfopropylgroups,5to10&

[note—AvailableasTSKICSWCationfromTosohBiosep（）.]

L53—Weakcation-exchangeresinconsistingofethylvinylbenzene,55%cross-linkedwithdivinylbenzenecopolymer,3to15&

mdiameter.Substrateissurfacegraftedwithcarboxylicacidand/orphosphoricacidfunctionalizedmonomers.Capacitynotlessthan500&

Eq/column.

[note—AvailableasIonPacCS14distributedbyDionexCorp.（）.]

L54—Asizeexclusionmediummadeofcovalentbondingofdextrantohighlycross-linkedporousagarosebeads,about13&

[note—AvailableasSuperdexPeptideHR10/30fromAmershamPharmaciaBiotech（）.]

L55—Astrongcation-exchangeresinmadeofporoussilicacoatedwithpolybutadiene–maleicacidcopolymer,about5&

[note—AvailableasIC-PakCM/DfromWatersCorp.（）.]

L56—Propylsilanechemicallybondedtototallyporoussilicaparticles,3to10&

[note—AvailableasZorbaxSB-C3fromAgilentTechnologies（

L57—Achiral-recognitionprotein,ovomucoid,chemicallybondedtosilicaparticles,about5&

mindiameter,withaporesizeof120.

[note—AvailableasUltronES-OVMfromAgilentTechnologies（

L58—Strongcation-exchangeresinconsistingofsulfonatedcross-linkedstyrene-divinylbenzenecopolymerinthesodiumform,about6to30&

m1S（USP31）indiameter.

[note—AvailableasAminexHPX-87NfromBio-RadLaboratori