TU1810紫外分光光度计说明书完整WORD版Word文档格式.docx
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1
.1部件的验收......................................................................1-1
.2主机各部分的说明................................................................1-1
.2.1主机正面...............................................................1-1
.2.2主机后面...............................................................1-1
.2.3显示器(TU-1810/TU-1810S).............................................1-2
.2.4键盘...................................................................1-3
1.3仪器规格........................................................................1-4
第2章仪器安装.........................................................2-1
2
.1安装场所........................................................................2-1
.2安装............................................................................2-1
.3开机............................................................................2-1
.4安装时的性能检查................................................................2-2
.4.1波长准确度与重复性.....................................................2-2
.4.2基线平直度.............................................................2-2
第3章光度测量.........................................................3-1
3
.1显示信息及功能键................................................................3-1
.2设定参数........................................................................3-1
.2.1设定测光方式...........................................................3-2
.2.2设定测量波长...........................................................3-2
.2.3输入K系数值...........................................................3-2
.2.4暗电流校正.............................................................3-3
.2.5退出参数设置...........................................................3-3
.3设定工作波长....................................................................3-3
.4试样控制........................................................................3-4
.4.1选择试样室类型.........................................................3-4
.4.2设定使用试样池数.......................................................3-4
.4.3一号池空白校正.........................................................3-5
.4.4移动试样池.............................................................3-5
.4.5试样池复位.............................................................3-5
.4.6单池测样...............................................................3-5
.4.7退出试样控制...........................................................3-5
.5自动校零(校100%T)............................................................3-5
.6测量............................................................................3-5
.6.1测量...................................................................3-6
.6.2测量结果的查阅.........................................................3-6
.6.3清除测量数据...........................................................3-6
.6.4打印...................................................................3-7
.6.5退出测量...............................................................3-7
第4章光谱测量.........................................................4-1
4.1显示信息及功能键................................................................4-1
4.2设定参数........................................................................4-1
4
.2.1设定测光方式...........................................................4-2
.2.2设定扫描速度...........................................................4-2
.2.3设定采样间隔...........................................................4-2
.2.4输入波长范围...........................................................4-2
.2.5输入测光值坐标范围.....................................................4-2
.2.6暗电流校正.............................................................4-3
.2.7退出参数设置...........................................................4-3
.3基线校正........................................................................4-3
.4测量............................................................................4-3
.5峰值检出........................................................................4-4
.6测量结果的打印..................................................................4-4
.7退出光谱扫描功能................................................................4-5
第5章定量测定.........................................................5-1
5
.1显示信息及功能键................................................................5-1
.2设定测量参数....................................................................5-1
.2.1设置定量测定法.........................................................5-2
.2.2设定测量波长...........................................................5-2
.2.3设定浓度单位............................................................5-2
.2.4暗电流校正.............................................................5-2
.2.5设定工作曲线参数(系数法).............................................5-2
.2.6设定工作曲线参数(标样法).............................................5-4
.3设定当前波长....................................................................5-6
.4自动校零........................................................................5-7
.5测量............................................................................5-7
.6测量结果的查阅..................................................................5-7
.7测量结果的打印..................................................................5-7
.8退出测量........................................................................5-7
第6章DNA/蛋白分析.....................................................6-1
6
.1显示信息及功能键................................................................6-1
.2设定测量参数....................................................................6-1
.2.1设置DNA/蛋白分析方法...................................................6-2
.2.2设定测量波长...........................................................6-2
.2.3设定DNA系数...........................................................6-2
.2.4设定蛋白质系数.........................................................6-3
.2.5设定320nm背景校正.....................................................6-3
.2.6设定校正系数...........................................................6-3
.3暗电流校正......................................................................6-4
.4退出DNA/蛋白质参数设置.........................................................6-4
.5自动校零........................................................................6-4
.6测量............................................................................6-4
.7测量结果的查阅..................................................................6-4
6.8测量结果的打印..................................................................6-5
6.9退出测量........................................................................6-5
第7章系统应用.........................................................7-1
7
.1显示信息及功能键................................................................7-1
.2设定换灯波长....................................................................7-1
.3设定仪器狭缝(该选项尽限于1810S型号)..........................................7-1
.4设钨灯开关......................................................................7-2
.5设氘灯开关......................................................................7-2
.6设工作模式......................................................................7-2
.7时间设置........................................................................7-2
.8暗电流校正......................................................................7-2
.9波长校正........................................................................7-3
.10退出系统应用...................................................................7-3
第8章日常保养与维修...................................................8-1
8
.1注意事项........................................................................8-1
.2日常保养........................................................................8-1
.3故障诊断与维修..................................................................8-1
8.3.1仪器初始化诊断.........................................................8-1
8.4灯源更换方法....................................................................8-2
.4.1更换钨灯...............................................................8-2
.4.2更换氘灯...............................................................8-3
第1章仪器简介
1.1部件的验收
打开仪器的包装后,请对照装箱单对仪器的齐套性进行认真清点、验收,如与装箱单不符或损
坏者,请及时与售方联系,以便尽快解决,仪器成套性如表1-1所示,以后如有更改均以装箱单为
准。
表1-1仪器的成套性
序号
名
称
数量
1台
1张
2张
1对
2只
2把
各2只
1个
9
紫外可见分光光度计主机
合格证
安装验收单
石英比色皿
溴钨灯
十字镙丝刀
一字镙丝刀
保险管(2A、0.5A)
内六方扳手
电源线
1条
1本
多用电源盒
装箱单
1.2主机各部分的说明
.2.1主机正面
✧
液晶显示器:
为320×
240点阵的高分辨率液晶显示器,用于显示测量信息、参数、数据及谱图,
允许用户调节显示辉度。
(调节孔在键盘的左上角)。
键盘:
共有27个按键,用于控制和操作仪器。
样品室:
用于放置被测样品,并可配置自动八联样品池架或五联池作为选装附件。
图(1-1)仪器前视图
.2.2主机后面
-1
光源室:
内部装有钨灯(可见光区)和氘灯(紫外光区)测量时根据波长范围自动转换,光源灯
亮时会发烫,更换光源时应特别注意。
打印机接口:
可连接HP系列喷墨打印机。
RS-232接口:
1810PC/1810SPC仪器备有RS232接口,支持串行通讯。
具体软件设置及操作详见
UVWin5.0软件使用说明书。
图(1-2)仪器后视接口图
一体化电源开关:
用于接通和切断主机电源,包括电源插座,保险管座,开关。
电源插座连接220V、
50Hz交流电源,保险管使用直径5mm、长20mm、2A。
光源室罩:
为方便用户更换光源而设置,拆装时应特别注意灯的温度,以免烫伤。
排风扇:
排风扇孔为仪器散热排风孔,为便于仪器散热,仪器安放位置应距墙壁20~30厘米,以
免遮挡排风孔。
图(1-3)仪器后视图