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1、3.10. Sulfide Stress Cracking test 硫化物应力腐蚀开裂试验 53.11. Frequency of Sample取样频次 73.12. Size and Weight Tolerance 尺寸和重量公差 83.12.1. Tolerance of Pipe Body 管体公差 83.12.1.1 Plain-End Pipes (Before threading) 平端管(车丝前) 83.12.1.2 Finished Product 成品管 83.12.2. Size and Tolerance of coupling stock 接箍料尺寸与公差 93.1

2、2.3. Weight Tolerance 重量公差 93.13. Drift Mandrel Size 通径规尺寸 103.14. Hydrostatic Test 水压测试 103.15. Non Destructive Examination无损探伤 103.15.1. Visual inspection 目视检查 103.15.2. Pipe Body管体 103.15.3. Pipe ends 管端 113.15.4. NDT unit Calibration 探伤设备校样 113.15.5. WT measurement壁厚测量 123.15.6. Coupling Stock 接

3、箍料 123.15.7. Artificial reference indicators 人工参考缺陷 133.15.8. Imperfection prove up of pipe body and coupling stock 管体和接箍料的缺欠探明 133.16. Stencil and Stamping 喷标和打标 143.16.1. Plain-End Pipes (Before threading) 平端管(车丝前) 141. Scope范围This Quality Control Plan gives the acceptance / rejection criteria for

4、 the manufacturing, inspection and testing of the referenced order. 本质量计划书规定了封面所列产品订单的生产制造、检验和试验的接受/判废标准。Special criteria apply for the acceptance / rejection of the plain-end pipes before threading.对车丝前的平端管,施行特殊的接受/判废标准。2. Coverage包含范围This quality control plan is only suitable for the 9- 47.0PPF T9

5、5-1 Casing.本质量计划书只适用于9- 47.0PPF T95-1套管。Supplementary requirements 补充要求: SR16, SR15 3. Product Quality Specification产品质量标准3.1. General总体要求Casing manufactured by this plan shall conform to 9th edition of API SPEC 5CT.本计划针对的套管生产必须符合API SPEC 5CT第9版。3.2. Heat Treatment and Straightening Requirements 热处理

6、和矫直要求Full length Quenched and tempered, minimum tempering temperature is 649C.全长淬火和回火,最低回火温度649C。Pipes may be subjected to cold rotary-straightening if, subsequent to the cold rotary straightening operation, the pipe is heated to a minimum temperature of 480C for stress-relieving.管子可进行冷旋转矫直,但矫直后必须把管

7、子加热到480C以上进行应力消除处理。3.3. Material and Chemical Composition Requirements材料与化学成分要求 API 5CT Specification标准:GradeChemical Composition化学成分 weight% 重量%C 碳Mn锰Mo钼Cr铬Ni镍 P磷S硫MaxMinT95-10.351.200.850.151.500.400.990.0200.0103.4. Mechanical Property Requirements 机械性能要求钢级Yield Strength屈服强度 MPaTensile Strength抗拉

8、强度 MPaElongation伸长率 %MINMAX655758724E=1 944 Note注意: ACross sectional area of the tensile test specimen拉伸试验样的横截面积 mm2 UMinimum specified tensile strength规定的最小抗拉强度MPa 3.5. Charpy V-Notch Test (General Requirements) 夏比V型槽冲击试验 (总体要求) Coupling Stock接箍料Absorbed Energy吸收能 J 101055 T-10-23Average平均Individua

9、l Specimen单个试样Longitudinal纵向Transverse横向-2316 J(max 1 sample最多一个试样)Note注意: 1. The test temperature is 0C 3C. 试验温度是0C. 2. Critical thickness is 15.29 mm. 最大临界厚度为15.29 mm。 Pipe body管体(API 5CT SR16):Absorbed Energy吸收能 J 107.555 T-7-151510 J(max 1 sample3.6. Maximum Hardness最高硬度 The hardness numbers and

10、/or mean hardness numbers obtained shall be no more than 25.4HRC.测得的硬度值和/或平均硬度值应不超过25.4HRC。 Through-wall hardness 全壁厚硬度Products with mean Rockwell hardness number not exceeding 25.4 HRC are acceptable. If any hardness number from a single indentation exceeds 27.0 HRC, the length or piece shall be re

11、jected. Products with mean hardness numbers between 25.4 HRC and 27.0 HRC shall be retested.平均硬度值不超过HRC25.4的产品是可接受的。若任何单个压痕测得的硬度值超过HRC27.0,则该根管子或管件应拒收。平均硬度值介于HRC25.4和HRC27.0之间的产品应重新试验。 Pipe body管体One through-wall hardness test in one quadrant shall be made on each length from one end of the pipe.一个象

12、限的全壁厚硬度试验应从管端取样进行。 Coupling stock 接箍毛坯For thick-wall pipe used for making more than one coupling, through-wall hardness tests shall be made on each of two test rings, one from each end. Through-wall hardness tests shall be made in four quadrants.对于用来制造多个接箍的厚壁管,应从每根管的两端各取一个全壁厚硬度试验环进行试验。全壁厚硬度试验应在四个象限进

13、行。3.7. Hardness variation 硬度变化The difference between any two mean hardness numbers within one quadrant is no more than 3.0HRC for pipe body and no more than 6.0 for coupling stock.在一个象限内任意两个平均硬度值之差管体不超过HRC3.0,接箍料不超过HRC6.0。3.8. Hardenability 淬透性For each size, mass, chemical composition and austenitiz

14、e-and-quench combination, a through-wall hardness test shall be made on products after quenching and prior to tempering for each production run to characterize the hardening response. Mean hardness numbers shall equal or exceed the hardness corresponding to a minimum of 90% martensite, as determined

15、 by the following equation:HRCmin = 58 (% carbon) + 27对每一规格、重量、化学成分以及奥氏体化及淬火组合,全壁厚硬度试验应在每一生产流程的淬火后、回火前的产品上取样进行试验,以测定淬透性。平均硬度值应等于或大于90%马氏体硬度值,计算公式如下:3.9. Grain size 晶粒度Prior austenitic grain size shall be ASTM 5 or finer. (determined in accordance with ISO 643 or ASTM E112)原始奥氏体晶粒度应为ASTM 5级或更细(根据ISO

16、643或 ASTM E112)。3.10. Sulfide Stress Cracking test 硫化物应力腐蚀开裂试验For each heat, manufacturers shall demonstrate that the product meets or exceeds the minimum SSC threshold using one of the ANSI-NACE TM0177-96 test methods.对每一炉,厂家需要采用ANSI-NACE TM0177-96中的某一种试验方法,并出示证明产品符合或超过硫化物应力腐蚀开裂试验最小要求。The Minimum S

17、SC threshold value for ANSI-NACE TM0177-96 Method A (Smooth tensile) is equal 80% of minimum Yield Strength 524 MPA (76000 psi) for full-size (6.350.13 mm 0.2500.005 in. in diameter, by 25.4 mm 1 in. long) specimen.ANSI-NACE TM0177-96 方法A(光滑拉伸试验)最低SSC门槛值等于标准规定的最小屈服强度的80%,即对于全尺寸试样(直径6.350.13mm 0.2500

18、.005 in;长度25.4mm1 in)为524 MPA(76000 psi)。Test Solution A shall consist of an acidified, H2S saturated aqueous environment. The solution pH after H2S saturation but before contact with a test specimen is expected to range between 2.6 and 2.8. During the test, pH may increase but shall not exceed 4.0.

19、 If the solution-volume-to-specimen-surface-area ratios are maintained and steps are taken to exclude oxygen from the test cell as specified in this standard, the pH will not exceed this value.Test Solution A shall consist of 5.0 wt% NaCl and 0.5 wt% glacial acetic acid dissolved in distilled or dei

20、onized water. For example, 50.0 g of NaCl and 5.0 g of glacial acetic acid can be dissolved in 945 g of distilled or deionized water.A型试验溶剂须由酸化了的饱和H2S水介质构成。溶液中H2S达到饱和但还没接触试样时的pH值应在2.6到2.8之间。试验中,pH值允许增大但不应超过4.0。如果溶液容量与试样表面积之比保持稳定且按本标准中指出的方法排除了实验间中的氧气,pH值将不会超过此值。A型试验溶液应由5.0 wt% NaCl 和 0.5 wt%冰醋酸溶解于蒸馏水

21、或去离子水制成,如将50.0 g NaCl 和 5.0 g 冰醋酸溶于945 g 蒸馏水或去离子水。The test solution shall be maintained at 24 3 试验溶液应保持在24 The failure of material is either:a) Complete separation of the test specimen;b) Visual observation of cracks on the gauge section of the test specimen at 10 after completing the 720 hour test

22、duration. Investigative techniques employing metallograhy, scanning microscopy, or mechanical testing may be used to determine whether cracks on the gauge section are evidence of EC (EC environmental cracking includes SSC sulphide stress cracking, SCC stress corrosion cracking, or hydrogen stress cr

23、acking). If it is verified that the cracks are not EC, then the test specimen passes the test.If SSC test representing a heat fails to conform to the specified requirements, the manufacturer may elect to make re-tests on two additional test specimens from the same pipe.If all of the re-tests conform

24、 to the requirements, the heat shall be accepted.If one or more of the re-tests specimens fails to conform to the specified requirements, the heat shall be rejected.在下列情况中的任何一种试验失效为:a)试样完全断开。b)经过720小时的试验时间后,采用10倍的放大镜目测试样的受检部位的裂纹,使用金相显微镜、扫描显微镜、或机械试验检查技术来确定受检部位的裂纹是否属于EC所造成的。(EC的含义是环镜开裂,仅包括硫化物应力开裂、应力腐蚀

25、开裂、氢致开裂。)如果裂纹经确认不是环境开裂,则该试样通过试验。若代表一炉产品的抗硫化物应力开裂试验不符合规定要求,则制造厂可以从同一支管子上另外再取2个样进行复验。若所有试样复验均符合要求,则该炉管子合格。若复验用一个或多个试样不符合规定要求,则该炉管子应判废。3.11. Frequency of Sample取样频次Test item 测试项Name of product产品名称 Frequency of sample取样频次Chemical composition化学成分Ladle 熔炼Pipe Body and Coupling管体和接箍1/heat炉Product产品2/heat炉G

26、rain size determination 晶粒度测定Pipe body管体Each heat treatment campaign 每次热处理Coupling stock接箍料Hardenability test 淬透性试验Tensile test拉伸试验1/lot of 100pcs max 每批取一个样,每批最多100支管子1 for each piece每支取一个样Impact test冲击试验1/lot of 100pcs max每批取一个样,每批最多100支管子 Coupling stock接箍料Hardness test硬度试验1/each piece1 每根12/each

27、piece2 每根2SSC test试验Pipe body and coupling stock 管体和接箍料1/heat3 每炉取1支3The lengths for testing shall be selected at random.试验用管应随机抽取。Note注:1 Approximately 50 % of these test rings for through-wall hardness test on one quadrant shall be cut from the front ends and approximately 50 % from the back ends of the pipe.全壁厚单象限硬度试验的试样环有约50%的应取自管子的前端,而另一半应取自管子的后端。2 Two test rings for through-wall hardness tests on four quadrants, one from each end.两个全壁厚四象限硬度试验环,从每端各取一个。3 Three test s

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