aspenbatch间歇精馏模拟.docx

1、aspenbatch间歇精馏模拟Aspen 间歇精馏模拟教程Use this Getting Started section to become familiar with the steps to set up a batch simulation using Aspen Batch Modeler.You will be modeling a system to recover methanol from a mixture of methanol and water.The objective is to separate methanol from the mixture with a

2、 purity of 99%. This mixture is not ideal given the polarity of the molecules; therefore, for a working pressure of 1atm, you will choose NRTL to model its physical properties.There are four steps in this process. Click a step to go the instructions for the step. Step 1 Set up the Properties for Asp

3、en Batch ModelerStep 2 Enter structural data and specifications for the Aspen Batch Modeler block Step 3 Enter Operating StepsStep 4 Run the simulation and view the resultsStep 1 - Set up the Properties for Aspen Batch ModelerWe want to define a Properties file that has the following defined.Compone

4、nts Property MethodWater NRTLMethanolTo define this Properties file, follow the steps below.To set up the Problem Definition file from within Aspen Batch Modeler:1.Start Aspen Batch Modeler.2.On the Species form, click Edit Using Aspen Properties.This will start Aspen Properties.3. Enter the Compone

5、nts:Component IDComponent nameFormulaWATERWATERH2OMETHANOLMETHANOLCH4OTip: You can use the Next button4. Click the Next button Properties Specifications form.5. On the Properties Specifications form, in the Property method field, select NRTL. Tip: Clicking the pull-down arrow on the field and typing

6、 N (the first letter of the propertymethod name) takes you to the right choice much faster than just scrolling down the long list.6. Click NextYou are taken to the binary parameters forms, where you can view the binary parameters that will be used for Properties Calculations.7. Click NextYou are pro

7、mpted to click one of the options shown below.8.There is no need for further input, so click OK to run the property setup.9.Close Aspen Properties by clicking File | Exit.You are prompted with the following:10. Click Yes to save the file.The Property setup is now complete.Step 2 - Enter structural d

8、ata and specifications for the Aspen Batch Modeler blockThe column has been designed as follows: Configuration10 Stages (this includes eight trays, condenser and pot) Vapor-liquid separationPot Geometry Elliptical head 1m diameter volume of 1m 3OverheadTotal CondenserDistillate mole flow rate = 4.5k

9、mol/hr Reflux drum is present(no need to enter dimension because we are defining fixed pressure profile/holdups; therefore reflux holdup will be entered)Pressure/Holdups Pressure profile is fixedCondenser pressure 1.01325 bar Column Pressure Drop 0.1 barHoldupsReflux Drum liquid holdup: 0.02 m3 Stag

10、e holdup: 0.005 m3Heat TransferDuty: 150 kWReceiversOne receiver for liquid distillate Initial condition: total reflux Initial ConditionsInitial Charge 18kmol of materialComponent mole fraction Methanol: 0.4Water: 0.6To Enter the Data1. Set the configuration to Batch Distillation Column, specify the

11、 number of stages and ensure valid phases are Vapor-Liquid on the Configuration Main form10 Stages (this includes eight trays, condenser, and pot) Vapor-liquid separation2. On the Setup | Pot Geometry tab , type the pot dimensions: Elliptical; 1m diameter; volume of 1m33.Click the Overhead form. On

12、the Condenser tab, click Total for Total condenser.4.On the Reflux tab, type the distillate mole flow rate:Distillate mole flow rate = 4.5kmol/hr Reflux drum is presentNote: You need not enter dimension because we are defining fixed pressure profile/holdups. Therefore, reflux holdup will be entered.

13、5. Click the Jacket Heating form under Setup. On the Jacket Heating tab, enter the pot conditions:Duty: 150 kW6.Click Pressure/Holdups | Pressure.7.On the Pressure tab, type the pressure profile: Pressure profile is fixed.Condenser pressure 1.01325 bar Column Pressure Drop 0.1 bar8. On the Holdups t

14、ab, type the reflux and stage holdup information:3Reflux Drum liquid holdup: 0.02 m Stage holdup: 0.005 m 39.Click Receivers | Distillate.10.On the Distillate tab, define one liquid distillate receiver.11.Click Initial Conditions | Main.12.On the Main tab, in the Initial condition field, click Total

15、 reflux.13. On the Initial Charge tab, define the following: Total initial charge: 18 kmol of material Component mole fraction:Methanol: 0.4Water: 0.6Note: Do not forget to save your work regularly.To save your file for the first time:1. On the File menu, click Save As.2. In the File name field, typ

16、e a name, or select a file name to overwrite an existing file:3. Click Save.Step 3 - Enter Operating StepsThere are two Operating Steps:1.Start product draw maintaining a distillate flow rate of 4.5 kmol/hr.2.Stop when the mole fraction of water in the distillate receiver approaches 0.01 from below.

17、 The batch is complete.To create the required operating steps to run the problem:1.Click Operating Steps and enter distil in the Name column of the Operating Steps table.This will create the first operating step distil.2. On the Changed Parameters tab, create an operating step to distill the methano

18、l by maintaining a distillate flow rate of 4.5 kmol/hr.3. On the End Condition tab, specify as the end condition the mole fraction of water in the distillate receiver approaching the value of 0.01 from below.Step 4 - Run the simulation and view the resultsThe simulation is now ready to run.Before ru

19、nning the simulation, it is a good idea to create plots for key variables such as: the composition and holdup in the Receiverthe composition and temperature in the pot and so onTo create plots for key variables:1. On the Plots form, click the Temperature and Composition to create time plots for pot

20、temperature and mole fractions.2. Use the Custom plots feature to create plots of the receiver holdups and compositions. Click New on the Custom plots table and specify H2O_distil as the name of the plot.3. Go to the Holdups Summary ResultsDistillate tab. Select the field that displays the WATER mol

21、e fraction and drag it on to the plot (H2O_distil) created in the previous step.4.Use the same approach to create plots of holdups in the receiver and/or the plot.5.You can change the time units displayed in the plots by clicking the Run Options toolbarbutton Select the time units in which the user

22、interface should display time field.14. Click the Run button and view the Simulation Messages window for any relevantmessages.Once the problem has run successfully you can view results in the forms.Batch time: 1.49 hours/ 89.4 minutes Pot temperature: 101.05 Methanol recovery: 6.636 kmolNote: It is always good practice to restart your simulation in order to restore it to time zero before saving your work.