ASTMD335909标准试验方法胶带法测量附着力.docx

1、ASTMD335909标准试验方法胶带法测量附着力Designation: D 3359 02名称： D 3359-02Standard Test Methods forMeasuring Adhesion by Tape Test1ASTM D3359-09 标准试验方法 胶带法测量附着力This standard is issued under the fixed designation D 3359; the number immediately following the designation indicates the year oforiginal adoption or, in

2、 the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon indicates an editorial change since the last revision or reapproval.这个标准是D 3359确定了以后发行的。数字代表名称最初通过的时间,或者修订情况,和最新版本。括号内的数字代表最新重新审批时间。上标代表最新版本的变化或重新审批。This standard has

3、 been approved for use by agencies of the Department of Defense.该标准已经被国防机构部门批准使用。1. Scope X围1.1 These test methods cover procedures for assessing theadhesion of coating films to metallic substrates by applying andremoving pressure-sensitive tape over cuts made in the film.本标准提出的试验方法是规定通过在漆膜切割区施加和撕离压

4、敏胶带的方式,对漆膜与金属底材之间的附 着力进行评定的程序1.2 Test Method A is primarily intended for use at job siteswhile Test Method B is more suitable for use in the laboratory.Also, Test Method B is not considered suitable for films thickerthan 5 mils .试验方法A主要是供工作场所用,而试验方法B更适合实验室使用。试验方法B被视为不适合厚度超过 5毫英寸125微米的漆膜。NOTE 1Subjec

5、t to agreement between the purchaser and the seller,Test Method B can be used for thicker films if wider spaced cuts are employed.注 1-根据买卖双方的协议,如果切割间距较宽,漆膜较厚时可采用试验方法B。1.3 These test methods are used to establish whether theadhesion of a coating to a substrate is at a generally adequatelevel. They do

6、 not distinguish between higher levels ofadhesion for which more sophisticated methods of measurementare required.本标准规定的试验方法用于总体判定涂层与底材之间的附着力是否达到足够的水平。如果附着力较高,本标准规定的试验方法无法精确地区分附着力的差别,需要使用更精确的测量方法。NOTE 2It should be recognized that differences in adherability of thecoating surface can affect the resu

7、lts obtained with coatings having thesame inherent adhesion.注2-应该注意到,涂层内在附着力相同的情况下,涂覆面附着性的差别会影响测量结果。1.4 In multicoat systems adhesion failure may occur betweencoats so that the adhesion of the coating system to thesubstrate is not determined.多层涂层体系可能出现层间脱落,无法确定涂层体系与底材之间的附着力。1.5 The values stated in

8、SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.SI单位的数值被视为标准,括号内的数值仅供参考.1.6 This standard does not purport to address the safetyconcerns, if any, associated with its use. It is the responsibilityof the user of this standard to establish appropriate

9、 safety andhealth practices and determine the applicability of regulatorylimitations prior to use.本标准并没有指出与其使用相关的所有安全事项。本标准的用户应负责在使用之前采取适当的安全和卫生 措施,并确定各项管理限制条件的适用性2. Referenced Documents 参考文件2.1 ASTM Standards: 美国材料与试验协会标准D 609 Practice for Preparation of Cold-Rolled Steel Panelsfor Testing Paint, V

10、arnish, Conversion Coatings, andRelated Coating Products2D609-涂料,清漆,转化涂层和相关覆层产品的测试-用冷轧钢板制备的标准实施规XD 823 Practices for Producing Films of Uniform Thicknessof Paint, Varnish, and Related Products on Test Panels2D823-色漆,清漆,喷漆与有关产品制成厚度均匀漆膜试片的方法D 1000 Test Method For Pressure-Sensitive Adhesive-Coated Tap

11、es Used for Electrical and Electronic Applications3D1000-电气设备用压合敏感胶粘剂涂覆带的试验方法D 1730 Practices for Preparation of Aluminum andAluminum-Alloy Surfaces for Painting4D1730- 涂漆用铝和铝合金表面预处理标准实施规XD 2092 Guide for Preparation of Zinc-Coated Steel Surfaces for Painting5D2092-用于涂漆的镀锌钢材表面预处理的标准指南D 2370 Test Met

12、hod for Tensile Properties of OrganicCoatings2D2370-有机涂层抗拉性能的标准试验方法。D 3330 Test Method for Peel Adhesion of Pressure-Sensitive Tape 6D3330- 压敏胶带剥离强度测试标准D 3924 Specification for Standard Environment for Conditioningand Testing Paint, Varnish, Lacquer, and RelatedMaterials2D3924-色漆,清漆,喷漆和相关物质状态调节和试验用标

13、准环境规XD 4060 Test Method for Abrasion Resistance of OrganicCoatings by the Taber Abraser2D4060 -用泰伯尔磨蚀机测定有机涂层耐磨性的标准试验方法3. Summary of Test Methods 试验方法摘要3.1 Test Method AAn X-cut is made through the film tothe substrate, pressure-sensitive tape is applied over the cut andthen removed, and adhesion is

14、assessed qualitatively on the 0to 5 scale.试验方法A：一个X切口贯通漆膜和底材 ,在切口处施加和移除压敏胶带,粘附力按照0-5等级进行评估。3.2 Test Method BA lattice pattern with either six oreleven cuts in each direction is made in the film to thesubstrate, pressure-sensitive tape is applied over the lattice andthen removed, and adhesion is eval

15、uated by comparison withdescriptions and illustrations.试验方法B：在涂层与底材之间切割出六道或十一道格形状的切痕,在格之间施加和移除压敏胶带,通过图表描述对比来评估粘附力。4. Significance and Use 意义和用途4.1 If a coating is to fulfill its function ofprotecting ordecorating a substrate, it must adhere to it for the expectedservice life. Because the substrate a

16、nd its surface preparation have a drastic effect on the adhesion of coatings,a method to evaluate adhesion of a coating to differentsubstrates or surface treatments, or of different coatings to thesame substrate and treatment, is of considerable usefulness inthe industry.如果涂层能保护或装饰底材,必须要达到预期的服务寿命。因为

17、涂层的附着性对底材和其表面处理或缺乏有强烈的影响,用同一种方法来评估不同底材涂层或表面处理,或同一底材和表面处理但不同涂层被视为无用1 These test methods are under the jurisdiction of ASTM Committee D01 onPaint and Related Coatings, Materials, and Applications and are the directresponsibility of Subcommittee D01.23 on Physical Properties of Applied PaintFilms.Curre

18、nt edition approved Aug. 10, 2002. Published October 2002. Originallypublished as D 3359 74. Last previous edition D 3359 97.2Annual Book of ASTM Standards, Vol 06.01.3Annual Book of ASTM Standards, Vol 10.01.4Annual Book of ASTM Standards, Vol 02.05.5Annual Book of ASTM Standards, Vol 06.02.6 Annua

19、l Book of ASTM Standards, Vol 15.09.此测试方法在美国材料与试验协会D01是关于油漆和相关涂层、材料、应用软件和关于油漆涂层的物理性能D01.23的权限下进行的。最新版本在20xx8月10号被认可。20xx10月出版。最初出版是D3359-74,上一个版本是D3359-97。4.2 The limitations of all adhesion methods and the specificlimitation of this test method to lower levels of adhesion should be recognized befor

20、e using it. The intra- andinter-laboratory precision of this test method is similar to otherwidely-accepted tests for coated substrates , but this is partly theresult of it being insensitive to all but large differences inadhesion. The limited scale of 0 to 5 was selected deliberatelyto avoid a fals

21、e impression of being sensitive.在使用前,应承认所有附着力方法的局限性和这个试验方法对较低级附着力见1.3的特殊限制。内部多个实验室所进行的精密度的这种测试方法类似于其他已被广泛接受涂层测试,为避免敏感的假象而刻意限定0-5等级X围。TEST METHOD AX-CUT TAPE TEST 试验方法A：划X法胶带测试5. Apparatus and Materials 仪器和材料5.1 Cutting ToolSharp razor blade, scalpel, knife or othercutting devices. It is of particula

22、r importance that the cuttingedges be in good condition.切削刀具：锋利的刀片、手术刀、刀或者其他切削设备。5.2 Cutting GuideSteel or other hard metal straightedgeto ensure straight cuts.引导切割钢制或其他金属制的直尺或夹具来保证直线切割。5.3 Tape25-mm wide semitransparent pressuresensitivetape7 with an adhesion strength agreed upon by thesupplier and

23、 the user is needed. Because of the variability inadhesion strength from batch-to-batch and with time, it isessential that tape from the same batch be used when tests areto be run in different laboratories. If this is not possible, the testmethod should be used only for ranking a series of testcoati

24、ngs.胶带经供应商和用户同意的25mm宽的半透明的透明具有粘合力压敏胶粘带。因为粘合力是随着时间和批次不同是变化的,故各个实验室进行测试时所使用的胶带要是同一批次的。如果无法做到这一点,此测试方法应仅适用于一系列涂层测试的排名。5.4 Rubber Eraser, on the end of a pencil.铅笔一头的橡皮擦5.5 IlluminationA light source is helpful in determiningwhether the cuts have been made through the film to thesubstrate.照明灯源如手电筒当在漆膜与底

25、材之间开有切割时,光源是有很有帮助的。6. Test Specimens 试样6.1 When this test method is used in the field, the specimenis the coated structure or article on which the adhesion is to beevaluated.当这个试验方法在实地使用时,被测试的结构或物品上的粘附力都将要被评估。6.2 For laboratory use apply the materials to be tested topanels of the composition and sur

26、face conditions on which it isdesired to determine the adhesion.实验室使用申请材料进行试验,通过测试板的成份的和表面情况来评估附着力。NOTE 3Applicable test panel description and surface preparationmethods are given in Practice D 609 and Practices D 1730 and D 2092.备注3：适用的测试板描述和表面处理方法见D 609和D 1730、D 2092。NOTE 4Coatings should be appli

27、ed in accordance with PracticeD 823, or as agreed upon between the purchaser and the seller.备注4：涂层应按照D 823,或者买方和卖方之间所达成的协议。NOTE 5If desired or specified, the coated test panels may be subjectedto a preliminary exposure such as water immersion, salt spray, or highhumidity before conducting the tape t

28、est. The conditions and time ofexposure will be governed by ultimate coating use or shall be agreed uponbetween the purchaser and seller.备注5：如需要或已列明,规定,涂层测试板在进行测试前可能需先暴露于/ 如：浸在水中,盐雾或高湿度中。浸泡的时间和条件应取决于涂层产品的最终用途或者买方和卖方之间达成的协议。7. Procedure 程序7.1 Select an area free of blemishes and minor surfaceimperfec

29、tions. For tests in the field, ensure that the surface isclean and dry. Extremes in temperature or relative humiditymay affect the adhesion of the tape or the coating.在实地做此试验时,需确保试样涂层表面要清洁干燥。高温和高湿会影响胶带附着力。 For specimens which have been immersed: Afterimmersion, clean and wipe the surface with an app

30、ropriatesolvent which will not harm the integrity of the coating. Thendry or prepare the surface, or both, as agreed upon between thepurchaser and the seller.根据买方和卖方之间双方达成的协议,对于被浸泡的样件,浸泡完以后用适当的溶剂不能损害涂层擦净表面,然后让其干燥7.2 Make two cuts in the film each about 40 mm long that intersect near their middle wit

31、h a smaller angle ofbetween 30 and 45. When making the incisions, use thestraightedge and cut through the coating to the substrate in onesteady motion.用刀具沿直线稳定地切割漆腊至底材,夹角30-45,划线40mm长,交叉点在线长的中间7.3 Inspect the incisions for reflection of light from themetal substrate to establish that the coating fil

32、m has beenpenetrated. If the substrate has not been reached make anotherX in a different location. Do not attempt to deepen a previouscut as this may affect adhesion along the incision.用灯光照明查看钢质基底的反射,确定划痕是否到底材,如果没有,在不同位置再划一个X。不要试图加深以前切口的深度,这样可能影响切口处的附着性。7.4 Remove two complete laps of the pressure-sensitivetap