冻干机手动和自动操作指南资料讲解.docx

1、冻干机手动和自动操作指南资料讲解5.1. Freeze-drying Operation操作用户操作设备进行冻干程序操作Logging in control system is needed before operating the equipment. In the control system, freeze-drying process can be done through 2 methods. 操作用户若需要对设备进行操作需要先登入控制系统。在控制系统中对于冻干可通过2种方式来完成 Automatic Control自动控制 Manual Control手动控制5.1.1 Opera

2、tor runs automatic control to do freeze-drying operation操作用户运行自动控制进行冻干流程操作In automatic control, switch all the control components to automatic control status at first and then set the recipe parameters. After that, “START AUTO.” will appear. User clicks the “START AUTO.” button to start automatic pr

3、ogram. 在自动控制中需要先切换把所有的控制部件切换到自动控制状态，然后设置配方参数，当设置好配方参数后“开始自动”按钮会显示，用户点击“开始自动”按钮启动自动程序。Control components open and close automatically according to automatic program. At the meanwhile, status of “AUTO” on the right upper corner will become green and the interface switch button “FREEZE_DRYING” on the l

4、eft lower corner will also has small green frame. 自动程序运行后控制部件按程序自动运行开启和关闭，同时在界面右上角的”自动状态会显示绿色、左下角的“冻干”界面切换按钮也会有绿的小方框显示。The operation status of automatic program can be displayed by clicking the “Program” button on right lower part and switching to program operational status. 自动程序的运行状况可点击界面右下部分的“程序”按

5、钮切换到程序运行状态显示。5.1.2 Control Components Switch to Automatic Control Status控制部件切换到自动控制状态Click any control components on the interface and digital signature of components control will pop up. After entering the user name and password, component control picture will appear. Click “ALL THE COMPONENTS CHAN

6、GE TO AUTO MODE” button and all the components control turn to automatic model. Users can find out status switch from the status icon beside components picture on the interface.点击界面的任何控制部件会弹出部件控制的电子签名，输入操作用户和密码后显示部件的控制画面，点击”全部切换为自动”按钮后所有的控制部件切换为自动模式，用户可从界面部件画面旁的状态图标可看出状态的切换。5.1.3 Recipe Parameters S

7、etting设置配方参数Before running the automatic programs, recipe parameters should be set and downloaded to the PLC in order to run the program according to designed process. If above operation will not be done, “START AUTO.” button will not display and automatic program will not start. 在运行自动程序前需要设定配方参数并且下

8、载到可编程控制器里（PLC）以让程序按设好的工艺进行运行，若不进行上述操作则“自动”按钮不会显示，自动程序也将无法启动。1. . Operation Buttons操作按钮No.Button Name 按钮名称Button Instructions按钮说明1View查看View the recipe配方的查看2Modify修改Modify the recipe配方的修改3New新建Build new recipe, new recipe name should be entered before building. 配方的新建，在新建配方前需要输入新配方名4Save保存Save the rec

9、ipe. Relevant recipes should be saved in the computer after modification for freeze-drying operation at next time. 配方的保存，在修改配方后需要对相应的配方进行保存操作，保存到电脑系统中以供下次冻干操作使用5Download下载Recipe downloading. Download the recipe to PLC in order to provide parameters for automatic program running of freeze-drying.配方的下

10、载，使配方数据下载到可编程控制器里供冻干自动程序运行提供参数。6Print打印Printing the recipe through printer output配方的打印，通过打印机输出7Delete删除Delete the recipe. This operation is not advised even unreasonable recipe exists. 配方的删除，此操作不建议使用，即使有不合理的配方也不建议删除操作2. Parameters Instruction参数说明Control process of freeze-drying is divided into 4 par

11、ts including Freezing Control (Program Section 16), Condenser Freezing (Program Section7, 8), Primary Drying (Program Section 919), and Drying Analysis (Program Section 2023). The 9th step section in Primary Drying is pre-vacuumizing phase and in this phase warming-up control will not be done. The t

12、emperature to be set should be consistent with the temperature setting value in the 6th step section. Each step section can include temperature setting, vacuum setting, and vacuum control choice and pressure-up control choice according to control requirements. 冷冻干燥控制流程分为4部分包括预冷(程序段16段)、后箱冷却(程序段7、8段)

13、、第一次升华干燥(程序段919段)、解析干燥 (程序段2023段)，升华干燥中的第9步段是预抽真空的阶段，此阶段不进行升温控制，设置的温度需要和第6步段的温度设定值一致，每个步段按控制需求可包括温度设置、真空设置、真空控制选择和压力升控制选择。Freezing Control part does not include vacuum setting, vacuum control choice and pressure-up control choice. The 7th step section in Condenser Freezing part is condenser temperat

14、ure setting and the 8th step section is maintaining time after condenser temperature is reached(at least set 20min). 预冷部分不包含真空设置、真空控制选择和压力升控制选择。后箱冷却部分第7步段是后箱温度设置，第8步段是达到后箱温度后维持的时间（至少设置20分钟）。The 9th step section in Primary Drying is pre-vacuumizing phase and in this phase warming-up control will not

15、be done. The temperature to be set should be consistent with the temperature setting value in the 6th step section. If choose pressure-up control button in the 19th step section, the pressure-up control will starts after the 19th step section and this control includes 2 parameter test time and press

16、ure-up setting value.升华干燥中的第9步段是预抽真空的阶段，此阶段不进行升温控制，设置的温度需要和第6步段的温度设定值一致，若在第19步段行若选择压力升控制选择按钮，则在19步段结束后进行压力升控制，压力升控制包括2个参数:测试时间和压力升设定值。As the same with Primary Drying, if choose pressure-up control in the 23th step section in Drying Analysis part, the control will starts after the 23th step section and that control includes 2 parameter test time and pre